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近紅外光譜分析技術(shù)在植物蛋白飲料定量分析中的應(yīng)用

發(fā)布時(shí)間:2018-10-05 17:03
【摘要】:利用近紅外光譜分析技術(shù)對(duì)植物蛋白飲料中脂肪和可溶性固形物含量進(jìn)行定量分析。采用向后間隔偏最小二乘法(Bi PLS)、組合間隔偏最小二乘法(Si PLS)、遺傳偏最小二乘法(GA-PLS)、競(jìng)爭(zhēng)性自適應(yīng)重加權(quán)法(CARS)優(yōu)選波段,并結(jié)合偏最小二乘法(PLS)建立植物蛋白飲料中脂肪和可溶性固形物的定量分析模型。結(jié)果表明,4種方法對(duì)模型均有優(yōu)化效果,可提高模型的穩(wěn)定性和精準(zhǔn)性,其中GA-Bi PLS、GA-Si PLS優(yōu)化效果最為明顯,脂肪、可溶性固形物的決定系數(shù)R2分別達(dá)到了0.984、0.97和0.988、0.990,預(yù)測(cè)標(biāo)準(zhǔn)均方差(RMSEP)分別為0.026、0.030和0.170、0.155,相對(duì)分析誤差(RPD)分別為8.077、7.000和9.112、10.000。表明近紅外光譜技術(shù)作為一種快速、便捷的檢測(cè)手段,適用于植物蛋白飲料品質(zhì)的快速檢測(cè)分析。
[Abstract]:The content of fat and soluble solids in vegetable protein beverage was quantitatively analyzed by near infrared spectroscopy (NIR). The backward interval partial least squares (Bi PLS),) combined interval partial least squares (Si PLS),) genetic partial least squares (GA-PLS) method and competitive adaptive reweighting method (CARS) were used to optimize the band selection. The quantitative analysis model of fat and soluble solids in vegetable protein beverage was established by partial least square method (PLS). The results show that all of the four methods can improve the stability and accuracy of the model, and the optimization effect of GA-Bi PLS,GA-Si PLS is the most obvious. The coefficient of determination (R2) of soluble solids was 0.9840.97 and 0.9880.900.The standard mean deviation (RMSEP) of the prediction was 0.026 ~ 0.030 and 0.170 ~ 0.155, respectively. The relative analysis error (RPD) was 8.077 ~ 7.000 and 9.112 ~ 10.000, respectively. Near-infrared spectroscopy is a rapid and convenient method to detect and analyze the quality of vegetable protein beverage.
【作者單位】: 中國(guó)食品發(fā)酵工業(yè)研究院;東北農(nóng)業(yè)大學(xué)工程學(xué)院管理科學(xué)工程系;河北養(yǎng)元智匯飲品股份有限公司;紅牛維他命飲料有限公司;
【基金】:國(guó)家自然科學(xué)基金項(xiàng)目(31671937)
【分類號(hào)】:O657.33;TS275.4

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1 劉小力;;液相色譜法與氨基酸分析法測(cè)定食品中甘氨酸的比較研究[J];食品科學(xué);2012年18期

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