【摘要】：針對維吾爾藥材洋甘菊進行質(zhì)量標準研究,進一步完善洋甘菊的質(zhì)量控制體系為維吾爾醫(yī)用藥和研發(fā)提供技術(shù)支撐。采用薄層色譜(TLC)法對洋甘菊中木犀草素成分進行鑒別,按《中國藥典》方法檢測其顯微鑒別、水分、總灰分、含量測定(HPLC)、水溶性及醇溶性浸出物等含量。TLC斑點清晰,顯微專屬性強;10批不同產(chǎn)地市售的洋甘菊藥材測得水分范圍在7.18%~8.55%;總灰分范圍9.15%~24.50%;酸不溶性灰分范圍在0.717%~8.237%;浸出物范圍在21.62%~32.52%;HPLC測定了木犀草素含量在0.146~0.293μg/g之間。該研究為洋甘菊藥材的質(zhì)量標準提供了充分的數(shù)據(jù),薄層色譜鑒別斑點清晰、重現(xiàn)性好,顯微鑒別有明顯特征,為洋甘菊藥材進行質(zhì)量標準和合理開發(fā)提供理論數(shù)據(jù)奠定了基礎(chǔ)。
[Abstract]:To improve the quality control system of Chamomile for Uygur medicine, to provide technical support for Uygur medicine and research and development. Luteolin in chamomile was identified by thin layer chromatography (TLC) (TLC). The microscopical identification of luteolin in chamomile was determined by the method of Chinese Pharmacopoeia. The water content, total ash content, water solubility and alcohol-soluble extract of (HPLC), were determined. The water content of 10 batches of Chamomile sold in different producing areas was 8.55; the total ash was 9.15 ~ 24.50; the acid insoluble ash was 0.717 ~ 8.237; the extract was 21.62 ~ 32.52; the content of luteolin was between 0.1466 and 0.293 渭 g / g by HPLC. This study provided sufficient data for the quality standard of Chamomile, the identification spots of TLC were clear, the reproducibility was good, and the microscopic identification had obvious characteristics. It lays a foundation for the quality standard and reasonable development of chamomile.
【作者單位】： 新疆醫(yī)科大學(xué)附屬中醫(yī)醫(yī)院藥學(xué)部;武警新疆總隊醫(yī)院藥局;
【分類號】：R29

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