本文選題：朱砂根 + 高效液相色譜法　； 參考：《中國藥房》2017年30期

【摘要】：目的:建立苗藥朱砂根的高效液相色譜(HPLC)指紋圖譜。方法:采用HPLC法。色譜柱為Diamonsil C_(18),流動(dòng)相為甲醇-水(梯度洗脫),流速為1.0 mL/min,檢測波長為220 nm,柱溫為30℃,進(jìn)樣量為10μL。以11-O-(3′,4′,5′-三羥基沒食子酰基)-巖白菜素為參照,測定16批藥材樣品的HPLC圖譜,采用《中藥色譜指紋圖譜相似度評(píng)價(jià)系統(tǒng)》(2012版)進(jìn)行共有峰指認(rèn)和相似度評(píng)價(jià),并就指紋圖譜進(jìn)行聚類分析。結(jié)果:16批朱砂根藥材的HPLC圖譜有6個(gè)共有峰,其中8批藥材樣品的相似度均0.9;16批朱砂根藥材可聚為4類。結(jié)論:該研究所建指紋圖譜可為朱砂根藥材的鑒別和質(zhì)量評(píng)價(jià)提供參考。
[Abstract]:Objective: to establish a high performance liquid chromatography (HPLC) fingerprint of cinnabar root. Methods: HPLC method was used. The chromatographic column was Diamonsil Che _ (18), the mobile phase was methanol-water (gradient elution), the flow rate was 1.0 mL / min, the detection wavelength was 220nm, the column temperature was 30 鈩，

本文編號(hào)：1964720