本文選題：去滯散 + 枳殼　； 參考：《中國獸藥雜志》2017年12期

【摘要】：為了測定去滯散中枳殼的含量,采用C18柱(4.6 mm×150 mm,5μm),在室溫下,以乙腈-水(20∶80,用磷酸調(diào)節(jié)pH值至3)為流動相,283 nm為檢測波長,流速為1.0 m L/min,建立了反相高效液相色譜(RP-HPLC)測定方法。結(jié)果顯示,柚皮苷在0.08~4μg范圍內(nèi)線性關(guān)系良好,R~2=0.9999,回收率為94.4%~101.7%,RSD為2.23%;新橙皮苷在0.08~4μg范圍內(nèi)線性關(guān)系良好,R~2=0.9995,回收率為90.6%~100.0%,RSD為2.85%。本方法簡便、準(zhǔn)確、快速,可用于控制去滯散中枳殼的含量。
[Abstract]:In order to determine the content of Fructus aurantii in removing stagnation, C18 column (4.6 mm x 150 mm, 5 mu m), at room temperature, with acetonitrile water (20: 80, phosphoric acid adjusted pH value to 3) as the mobile phase, 283 nm as the detection wavelength and the velocity of 1 m L/min, a reversed phase high performance liquid chromatography (RP-HPLC) method was established. The results showed that naringin was in 0.08~4 mu g range. The system is good, R~2=0.9999, the recovery rate is 94.4%~101.7%, RSD is 2.23%. The linear relationship of new hesperidin in the range of 0.08~4 mu g is good, R~2=0.9995, the recovery rate is 90.6%~100.0%, RSD is 2.85%. this method is simple, accurate and fast. It can be used to control the content of Fructus aurantii in the stagnation.
【作者單位】： 中國農(nóng)業(yè)科學(xué)院蘭州畜牧與獸藥研究所;甘肅省獸藥飼料監(jiān)察所;
【基金】：公益性行業(yè)(農(nóng)業(yè))科研專項(項目編號:20130340-15)
【分類號】：S853.7

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