【摘要】：本研究著眼于確定制備純相Li Fe PO4脈沖激光沉積靶材的合成條件。通過(guò)TG-DTA實(shí)驗(yàn)分析合成過(guò)程,XRD檢測(cè)確定晶相,SEM觀察表面形貌。結(jié)果表明,采用液相法在800℃、通有氬氣(93%)和氫氣(7%)的混合氣體中焙燒制得純相的Li Fe PO4粉末,經(jīng)壓合焙燒獲得了純相、高結(jié)晶度、大晶粒的Li Fe PO4靶材。利用脈沖激光技術(shù)沉積Li Fe PO4薄膜,薄膜結(jié)構(gòu)致密,晶粒粒徑達(dá)納米級(jí)別。
[Abstract]:The purpose of this study is to determine the synthetic conditions for preparing pure Li Fe PO4 pulsed laser deposition targets. The surface morphology of crystal phase was determined by TG-DTA. The results showed that pure phase Li Fe PO4 powder was prepared by liquid phase roasting at 800 鈩，

本文編號(hào)：2259044