采用新型混合模式色譜柱HPLC法測定利伐沙班中殘留的乙酸
發(fā)布時間:2019-05-09 22:56
【摘要】:采用新型混合模式色譜柱Dionex Acclaim汶Mixed-Mode WAX-1,建立了高效液相色譜法測定利伐沙班中的殘留溶劑乙酸。流動相為乙腈∶0.025 mol/L磷酸二氫鉀溶液(50∶50),檢測波長為210 nm,以外標法計算。乙酸在1~10μg/ml范圍內(nèi)線性關(guān)系良好,平均回收率為100.6%,RSD為0.10%。
[Abstract]:High performance liquid chromatography(HPLC)was established for the determination of residual solvent acetic acid in rivaroxaban by means of a new mixed mode chromatographic column Dionex Accaimwen Mixed ModeWAX1. The mobile phase was acetonitrile鈭,
本文編號:2473153
[Abstract]:High performance liquid chromatography(HPLC)was established for the determination of residual solvent acetic acid in rivaroxaban by means of a new mixed mode chromatographic column Dionex Accaimwen Mixed ModeWAX1. The mobile phase was acetonitrile鈭,
本文編號:2473153
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