Gd離子注入對固溶態(tài)Mg-Nd-Sr-Zr合金生物腐蝕行為的影響
發(fā)布時間:2018-07-20 11:44
【摘要】:對固溶態(tài)Mg-Nd-Sr-Zr合金進行了釓(Gd)離子注入改性處理;采用SRIM 2008軟件對Gd離子注入過程進行了模擬分析;采用光學顯微鏡(OM)觀察了鎂合金的顯微組織,并利用X射線衍射儀(XRD)分析改性層中的物相組成,同時結(jié)合X射線光電子能譜(XPS)表征改性層中化學成分與元素價態(tài),采用電化學實驗及析氫實驗評價了基體鎂合金與注入鎂合金在模擬體液(SBF)中的生物腐蝕行為。結(jié)果表明:Gd離子注入有助于提高固溶態(tài)Mg-Nd-Sr-Zr合金在SBF中耐生物腐蝕性能,且當注入劑量為2.5×10~(16)cm~(-2)時,注入鎂合金的耐生物腐蝕性能最佳。
[Abstract]:The solid solution Mg-Nd-Sr-Zr alloy was modified by gadolinium ion implantation, the process of Gd ion implantation was simulated and analyzed by SRIM 2008 software, and the microstructure of magnesium alloy was observed by optical microscope (OM). The phase composition of the modified layer was analyzed by X-ray diffractometer (XRD), and the chemical composition and the valence state of elements in the modified layer were characterized by X-ray photoelectron spectroscopy (XPS). The biocorrosion behavior of magnesium alloy matrix and implanted magnesium alloy in simulated body fluid (SBF) was evaluated by electrochemical and hydrogen evolution experiments. The results show that the biological corrosion resistance of Mg-Nd-Sr-Zr alloy in SBF can be improved by the implantation of W Gd ion, and when the implantation dose is 2.5 脳 10 ~ (16) cm ~ (-2), the biocorrosion resistance of the implanted magnesium alloy is the best.
【作者單位】: 南京工程學院材料工程學院;南京工程學院江蘇省先進結(jié)構(gòu)材料與應用技術(shù)重點實驗室;
【基金】:國家自然科學基金資助項目(51301089) 江蘇省“青藍工程”資助項目~~
【分類號】:TG146.22;R318.08
本文編號:2133409
[Abstract]:The solid solution Mg-Nd-Sr-Zr alloy was modified by gadolinium ion implantation, the process of Gd ion implantation was simulated and analyzed by SRIM 2008 software, and the microstructure of magnesium alloy was observed by optical microscope (OM). The phase composition of the modified layer was analyzed by X-ray diffractometer (XRD), and the chemical composition and the valence state of elements in the modified layer were characterized by X-ray photoelectron spectroscopy (XPS). The biocorrosion behavior of magnesium alloy matrix and implanted magnesium alloy in simulated body fluid (SBF) was evaluated by electrochemical and hydrogen evolution experiments. The results show that the biological corrosion resistance of Mg-Nd-Sr-Zr alloy in SBF can be improved by the implantation of W Gd ion, and when the implantation dose is 2.5 脳 10 ~ (16) cm ~ (-2), the biocorrosion resistance of the implanted magnesium alloy is the best.
【作者單位】: 南京工程學院材料工程學院;南京工程學院江蘇省先進結(jié)構(gòu)材料與應用技術(shù)重點實驗室;
【基金】:國家自然科學基金資助項目(51301089) 江蘇省“青藍工程”資助項目~~
【分類號】:TG146.22;R318.08
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1 邢曉夏,劉均洪;生物腐蝕的研究進展[J];化學工業(yè)與工程技術(shù);2005年02期
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