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表面金屬化稻殼基陶瓷顆粒制備及其摩擦學(xué)性能研究

發(fā)布時(shí)間:2019-05-11 23:03
【摘要】:稻殼基陶瓷顆粒(RHC)是實(shí)現(xiàn)稻殼綜合利用的有效途徑之一,采用常規(guī)化學(xué)鍍方法將稻殼基陶瓷顆粒進(jìn)行化學(xué)鍍鎳,可擴(kuò)展其應(yīng)用范圍。利用單因素和正交實(shí)驗(yàn),確定了鍍鎳的最佳工藝參數(shù),將表面鍍鎳稻殼基陶瓷顆粒添加入鋁基材料中,研究對(duì)復(fù)合材料的抗磨減摩特性的影響。利用X射線衍射儀和高分辨率透射電鏡等分析手段對(duì)鍍鎳稻殼基陶瓷顆粒進(jìn)行了表面分析。結(jié)果表明,稻殼基陶瓷顆粒表面鍍鎳的最佳工藝為,溫度為60℃、時(shí)間為180min、鍍液pH值為11以及次亞磷酸鈉濃度為180g/L。稻殼基陶瓷顆粒表面分布著大量直徑約為40~50nm之間的鎳納米顆粒;鍍鎳的稻殼基陶瓷顆?擅黠@的改善鋁基材料的抗磨減摩特性。
[Abstract]:Rice husk based ceramic particle (RHC) is one of the effective ways to realize the comprehensive utilization of rice husk. The conventional Electroless plating method can expand the application range of rice husk based ceramic particles. The optimum technological parameters of nickel plating were determined by single factor and orthogonal experiments. The effect of adding nickel-coated rice shell based ceramic particles on the antiwear and antifriction properties of the composites was studied by adding nickel-coated rice shell based ceramic particles to aluminum-based materials. The surface of nickel-plated rice shell based ceramic particles was analyzed by X-ray diffractometer and high resolution transmission electron microscope. The results showed that the optimum conditions of nickel plating on the surface of rice husk based ceramic particles were as follows: temperature 60 鈩,

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