【摘要】：研究了致幻性安非他明類藥物3,4-亞甲二氧基甲基安非他明(MDMA)和3,4-亞甲二氧基安非他明(MDA)的乙�；�、三氟乙�；⑽宸；⑵叻□；⒍纫阴；⒁宦榷阴；⑽宸郊柞；⑽宸交酋；投趸郊柞；难苌磻�(yīng)條件,發(fā)現(xiàn)除了乙�；馑芯康母鞣N衍生化反應(yīng)均可用5μL酸酐或酰氯在環(huán)己烷中于20℃10 m in內(nèi)完成。乙�；捎�20μL乙酸酐在60℃30 m in內(nèi)完成。在此基礎(chǔ)上建立了尿中MDMA和MDA的各種衍生化的氮磷檢測氣相色譜(GC/NPD)分析方法。方法操作簡便快速,絕大多數(shù)方法的檢出限低于10μg/L,其中二氯乙�；�、一氯二氟乙酰化、五氟苯甲酰化、五氟苯磺酰
[Abstract]:The acetylation, trifluoroacetylation, pentafluoropropionylation, heptafluorobutyloylation and dichloroacetylation of the hallucinogenic amphetamines 3- (4-methylene) methamphetamine (MDMA) and 3- (4-methylenedioxyamphetamine) (MDA) were studied, Conditions for the derivatization of monochlorodifluoroacetylation, pentafluorobenzoylation, pentafluorobenzenesulfonylation and dinitrobenzoylation, It was found that all the derivation reactions except acetylation could be completed in cyclohexane at 20 鈩，

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