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抗高溫油基鉆井液主乳化劑的合成與評(píng)價(jià)

發(fā)布時(shí)間:2018-11-16 20:08
【摘要】:以妥爾油脂肪酸和馬來酸酐為主要原料合成了一種油基鉆井液抗高溫主乳化劑HT-MUL,并確定了妥爾油脂肪酸單體的最佳酸值及馬來酸酐單體的最優(yōu)加量對(duì)HT-MUL進(jìn)行了單劑評(píng)價(jià),結(jié)果表明HT-MUL的乳化能力良好,配制的油水比為60:40的油包水乳液的破乳電壓最高可達(dá)490 V,90:10的乳液破乳電壓最高可達(dá)1 000 V,從抗溫性、濾失性、乳化率方面對(duì)HT-MUL和國內(nèi)外同類產(chǎn)品進(jìn)行了對(duì)比,結(jié)果表明HT-MUL配制的乳液破乳電壓更大、濾失量更小、乳化率更高,整體性能優(yōu)于國內(nèi)外同類產(chǎn)品,應(yīng)用主乳化劑HT-MUL配制了高密度的油基鉆井液,其性能評(píng)價(jià)表明體系的基本性能良好,在220℃高溫?zé)釢L后、破乳電壓高達(dá)800 V,濾失量低于5 mL HT-MUL配制的油基鉆井液具有良好的抗高溫性和乳化穩(wěn)定性。
[Abstract]:A high temperature resistant main emulsifier HT-MUL, for oil based drilling fluid was synthesized from tul oil fatty acid and maleic anhydride as main raw materials. The optimum acid value of tul oil fatty acid monomer and the optimum addition amount of maleic anhydride monomer to HT-MUL were determined. The results showed that the emulsifying ability of HT-MUL was good. When the oil / water ratio is 60:40, the maximum demulsifying voltage of the emulsion with oil / water ratio of 60:40 can be up to 490 V / 90: 10. The highest demulsification voltage of the emulsion can be as high as 1 000 V, which can be obtained from the resistance to temperature and filtration. The emulsification ratio of HT-MUL is compared with that of the domestic and foreign products. The results show that the emulsion prepared by HT-MUL has higher demulsification voltage, less filtrate loss, higher emulsification rate and better overall performance than the domestic and foreign similar products. A high density oil-base drilling fluid was prepared by using the main emulsifier HT-MUL. The performance evaluation shows that the basic properties of the system are good, and the demulsification voltage is up to 800V after hot rolling at 220 鈩,

本文編號(hào):2336514

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