改性羧甲基纖維素高強(qiáng)度凝膠的制備及破膠性能研究
發(fā)布時間:2018-07-01 15:13
本文選題:改性CMC + 高強(qiáng)度凍膠; 參考:《現(xiàn)代化工》2017年12期
【摘要】:為滿足不壓井作業(yè)對凍膠新材料的性能要求,對羧甲基纖維素凝膠合成進(jìn)行了系統(tǒng)性的分析研究,制備出一種高強(qiáng)度、抗剪切、能夠?qū)崿F(xiàn)自破膠且破膠時間可控的改性羧甲基纖維素(CMC)智能膠體。該膠體的最優(yōu)質(zhì)量分?jǐn)?shù)分別為:水79.41%,CMC 1%,丙烯酰胺8%,NaCl 0.5%,固化劑0.45%,過硫酸銨0.02%,有機(jī)交聯(lián)劑0.02%,自制破膠劑10%,增黏劑0.6%。膠體最大本體強(qiáng)度可達(dá)44.5 N,最佳成膠溫度范圍為70~80℃,加入自制膠囊破膠劑后可實(shí)現(xiàn)38~70 h膠體的可控破膠,破膠殘液為深棕黃色液體,利于返排。
[Abstract]:In order to meet the performance requirements of the new gel material, the synthesis of carboxymethyl cellulose gel was studied systematically and a kind of high strength and shear resistance was prepared. The intelligent colloid of modified carboxymethyl cellulose (CMC) can be realized with self-breaking and controlled breaking time. The optimum mass fractions of the colloid were: water 79.41 and CMC 1, acrylamide 8 and NaCl 0.5, curing agent 0.45, ammonium persulfate 0.02, organic crosslinking agent 0.02, self-made gel breaking agent 10 and thickener 0.6. The maximum bulk strength of the colloid can reach 44.5 N, and the optimum gelation temperature range is 7080 鈩,
本文編號:2088188
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