基于氮?dú)馕?核磁共振-氬離子拋光場(chǎng)發(fā)射掃描電鏡研究川西須五段泥質(zhì)巖儲(chǔ)層孔隙結(jié)構(gòu)
本文選題:泥質(zhì)巖 切入點(diǎn):孔隙結(jié)構(gòu) 出處:《巖礦測(cè)試》2017年01期 論文類型:期刊論文
【摘要】:微觀孔隙作為泥質(zhì)巖的有效儲(chǔ)集空間,其孔隙結(jié)構(gòu)參數(shù)是作為氣藏評(píng)價(jià)及資源量估算的重要依據(jù)。本文應(yīng)用氮?dú)馕椒?NAM)、核磁共振法(NMR)、氬離子拋光及場(chǎng)發(fā)射掃描電鏡(AIP-FESEM)研究川西須五段泥質(zhì)巖微觀孔隙特征,結(jié)果表明:1氬離子拋光及場(chǎng)發(fā)射掃描電鏡在表征微觀孔隙形態(tài)與類別時(shí)有一定優(yōu)勢(shì),但定量表征孔隙參數(shù)時(shí),受圖像二值化閾值的影響,表征結(jié)果偏差較大,可結(jié)合氮?dú)馕椒▉?lái)定量表征其孔徑大小;2核磁共振受巖石骨架影響小,能夠更精細(xì)反映巖石的物性條件,可定量計(jì)算孔隙度與可動(dòng)流體飽和度,但對(duì)樣品的孔隙形態(tài)反映較差;3綜合上述三種方法,在須五段泥質(zhì)巖中可識(shí)別出一定量的納米級(jí)中、大孔,孔徑大多介于幾十納米到幾百納米之間,孔隙連通性差,孔隙度主要介于2.3%~7.4%之間,孔隙類型以粒間孔、晶間孔最發(fā)育,有機(jī)孔隙、微裂縫次之,粒內(nèi)孔隙最不發(fā)育?傮w而言,融合了三種技術(shù)方法能更精確、更全面地反映泥質(zhì)巖孔隙結(jié)構(gòu)特征,能得到更完善的儲(chǔ)層孔隙結(jié)構(gòu)參數(shù),在定量表征泥質(zhì)巖孔隙結(jié)構(gòu)中具有廣泛的應(yīng)用前景。
[Abstract]:As the effective reservoir micro pore argillaceous rock in space, the pore structure parameters is an important basis for the estimation of gas reservoir evaluation and amount of resources. In this paper the application of nitrogen adsorption method (NAM), nuclear magnetic resonance spectroscopy (NMR), argon ion polishing and field emission scanning electron microscopy (AIP-FESEM) to study the micro pore characteristics, five a mud rock shows: 1 argon ion polishing and field emission scanning electron microscopy has certain advantages in the characterization of pore morphology and category, but the quantitative characterization of pore parameters, the influence of threshold value of the two images, the characterization results of large deviation, can be combined with nitrogen adsorption method to quantitatively characterize the pore size of 2 nuclear magnetic resonance; the rock is small, can fine reflects the physical conditions, quantitative calculation of porosity and saturation of mobile fluid, but the pore morphology of the samples reflect the poor; 3 of the above three methods, in paragraph five shall argillaceous rock May be recognized in a certain amount of nano scale, big hole, aperture are range from tens of nanometers to hundreds of nanometers, pore connectivity, porosity is between 2.3%~7.4%, the pore types are mainly intergranular pore, intercrystalline pore and the development of organic pore, micro cracks of intragranular pore's development. Overall, the fusion of the three techniques can be more accurate, more fully reflect the pore structure characteristics of argillaceous rock, reservoir pore structure parameters can be more perfect, and has wide application prospect in the quantitative characterization of pore structure of mud.
【作者單位】: 中國(guó)石化西南油氣分公司勘探開發(fā)研究院;中國(guó)石化西南油氣分公司開發(fā)管理部;西南石油大學(xué)資源與環(huán)境學(xué)院;
【基金】:中石化西南分公司開發(fā)類支撐項(xiàng)目(GJ-332-1426)
【分類號(hào)】:P618.13
【相似文獻(xiàn)】
相關(guān)期刊論文 前1條
1 鮑芳;劉偉新;;中國(guó)石化無(wú)錫石油地質(zhì)研究所實(shí)驗(yàn)地質(zhì)技術(shù)之氬離子拋光分析技術(shù)[J];石油實(shí)驗(yàn)地質(zhì);2014年04期
相關(guān)會(huì)議論文 前1條
1 陳寧英;;等離子拋光在真空鍍膜前處理中的應(yīng)用[A];薄膜技術(shù)高峰論壇暨廣東省真空學(xué)會(huì)學(xué)術(shù)年會(huì)論文集[C];2009年
相關(guān)博士學(xué)位論文 前1條
1 王季;金屬表面電解質(zhì)等離子拋光及其工藝的研究[D];哈爾濱工業(yè)大學(xué);2013年
相關(guān)碩士學(xué)位論文 前4條
1 隗倩;基于小型電解等離子拋光機(jī)的鋁合金配方優(yōu)化及應(yīng)用研究[D];哈爾濱工業(yè)大學(xué);2015年
2 陳江波;大氣等離子拋光定量去除方法研究[D];哈爾濱工業(yè)大學(xué);2016年
3 薛浩;鋁合金的電解質(zhì)-等離子拋光工藝參數(shù)及試驗(yàn)裝置研究[D];哈爾濱工業(yè)大學(xué);2013年
4 趙培君;常溫大氣等離子拋光去除速度函數(shù)的研究[D];哈爾濱工業(yè)大學(xué);2009年
,本文編號(hào):1636481
本文鏈接:http://sikaile.net/kejilunwen/diqiudizhi/1636481.html