銅納米顆粒修飾柔性石墨構(gòu)建無酶葡萄糖傳感器(英文)
發(fā)布時間:2023-03-07 17:44
柔性石墨片(FGS)具備優(yōu)良的導(dǎo)電性與柔韌性,可作為葡萄糖傳感器的自支撐載體,解決由于使用黏結(jié)劑降低傳感器性能的問題。本文采用水熱法,使用抗壞血酸還原硫酸銅,在FGS上復(fù)合銅納米顆粒構(gòu)建Cu/FGS自支撐無酶葡萄糖傳感器,在線性范圍0.1~3.4 mmol/L內(nèi)具有較高的靈敏度7 254.1μA·mM-1·cm-2(R2=0.996 1),較低的檢測限1.05μmol/L;在線性范圍3.4~5.6 mmol/L靈敏度為3 804.5μA·mM-1·cm-2(R2=0.9995)。此外,該電極還有較好的抗干擾性、重復(fù)性及穩(wěn)定性。
【文章頁數(shù)】:10 頁
【文章目錄】:
1 Introduction
2 Materials and methods
2.1 Experimental materials and instruments
2.2 Experiment procedure
3 Results and discussion
3.1 Morphology and structure analysis of FGS
3.2 Morphology and structure analysis of FGS modified by copper nanoparticles (Cu/FGS)
3.2.1 Effect of the molar ratio of copper sulfate to ascorbic acid on the morphology and structure of Cu/FGS
3.2.2 Effect of the hydrothermal temperature on the morphology and structure of Cu/FGS
3.3 Electrochemical performance analysis of Cu/FGS
4 Conclusions
本文編號:3757606
【文章頁數(shù)】:10 頁
【文章目錄】:
1 Introduction
2 Materials and methods
2.1 Experimental materials and instruments
2.2 Experiment procedure
3 Results and discussion
3.1 Morphology and structure analysis of FGS
3.2 Morphology and structure analysis of FGS modified by copper nanoparticles (Cu/FGS)
3.2.1 Effect of the molar ratio of copper sulfate to ascorbic acid on the morphology and structure of Cu/FGS
3.2.2 Effect of the hydrothermal temperature on the morphology and structure of Cu/FGS
3.3 Electrochemical performance analysis of Cu/FGS
4 Conclusions
本文編號:3757606
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